Planetary Ball Milling
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Contents
General remarks
Selection of the milling media
Which balls to use? Material, size, quantity? Which jar to use? How much filling can go in? Which liquid to use?
Stoichiometry considerations
Weighting in the powder and milling balls
Milling procedure
Separating the slurry
Use a very clean sieve (sieves are a source of contamination) and a wide and clean glass beaker to separate the slurry and balls. The finer the balls are, the more slurry and powder remains in the balls. It can be drained with additional liquid.